Difference between revisions of "NMR"
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| − | + | === Notes === | |
* <span style="color: red; text-decoration: none; font-weight:bold; font-size: 14pt">WARNING: STRONG MAGNETIC FIELD!</span> | * <span style="color: red; text-decoration: none; font-weight:bold; font-size: 14pt">WARNING: STRONG MAGNETIC FIELD!</span> | ||
** <span style="color: red; text-decoration: none; font-weight:normal; font-size: 12pt">Read all warnings posted near instrument.</span> | ** <span style="color: red; text-decoration: none; font-weight:normal; font-size: 12pt">Read all warnings posted near instrument.</span> | ||
* The NMR has a hardware console. The PC connects to the NMR console via ethernet cable. | * The NMR has a hardware console. The PC connects to the NMR console via ethernet cable. | ||
| − | ** The PC is configured with a dedicated private [ | + | ** The PC is configured with a dedicated private [172.16.0.0/24] network on eth1/eno1. |
| − | ** | + | ** eth2/eno2 is on TESC LAN w/ static IP 10.15.10.6 |
* Student access to the PC: | * Student access to the PC: | ||
** UN: student | ** UN: student | ||
| − | ** PW: | + | ** PW: student1 |
* Network Information | * Network Information | ||
** PC is not joined to the domain; | ** PC is not joined to the domain; | ||
| − | + | ** There's a shortcut on the desktop [called NMR-Data] to \\Orca\research\NMR-Data [this is a 'static' connection using the scuser domain account] | |
| − | ** There's a | + | |
* The reference hardware/software serial #: S010780 | * The reference hardware/software serial #: S010780 | ||
| − | * The software ( | + | * The software (OpenVnmrJ) will create raw free induction decay [http://en.wikipedia.org/wiki/NMR_spectra_database#Raw_free_induction_decay '''(FID)''' ] files |
| − | + | ** These files can be directed to the network share by browsing to \Home\student\desktop\NMR-Data | |
| − | + | ||
| − | + | ||
| − | ** These files can be directed to the network share by browsing to \Home\student\desktop\NMR-Data | + | |
| − | + | ||
| − | + | ||
* VnmrJ Issues/Bugs: | * VnmrJ Issues/Bugs: | ||
** If the software is closed by clicking on the window x icon to close the application, VnmrJ will leave behind a lock file within the users profile. | ** If the software is closed by clicking on the window x icon to close the application, VnmrJ will leave behind a lock file within the users profile. | ||
| Line 40: | Line 35: | ||
*** the lock file will have a .primary file extension as well as having "lock" in the file name; | *** the lock file will have a .primary file extension as well as having "lock" in the file name; | ||
**** for example: rm_lock_4.primary | **** for example: rm_lock_4.primary | ||
| − | **** in the example, the 4 will represent the "4" or "4th" test. | + | **** in the example, the 4 will represent the "4" or "4th" test. |
| + | * Printer Configuration | ||
| + | ** printer setup within VNMRJ administration, requires that the printer be configured with emulation, specifically ''Laser Jet 600R'' has been found to be a good configuration that will utilize the entire 8 1/2 x 11 page for plotter. | ||
<br/> | <br/> | ||
| − | ====== | + | ==== '''General instrument information''' ==== |
| − | * Use [http://sourceforge.net/projects/gsim GSim] software for processing/analysis of FID files | + | * The helium needs to be recharged every 4 month [MAX believed to be 6 months] |
| + | * The liquid nitrogen needs to be recharged every 1 week [Max is believed to be 2 weeks] | ||
| + | * Consequence of failure to recharge aformentioned gases is [http://en.wikipedia.org/wiki/Magnet_quench#Magnet_quench "Magnetic Quench"!] | ||
| + | ** It's estimated that it would/will cost $15K to fix should quench occur. | ||
| + | <br/> | ||
| + | === NMR Spectroscopy Software === | ||
| + | * Use [http://sourceforge.net/projects/gsim GSim] software for processing/analysis of [http://en.wikipedia.org/wiki/NMR_spectra_database#Raw_free_induction_decay '''FID''' ] files | ||
** The [[CAL]] has GSim software installed. | ** The [[CAL]] has GSim software installed. | ||
| − | *** Former software used for trying to work with FID files --these are proprietary software: | + | *** Former software used for trying to work with [http://en.wikipedia.org/wiki/NMR_spectra_database#Raw_free_induction_decay '''FID''' ] files --these are proprietary software: |
**** <span style="text-decoration:line-through;">Acorn NMR Inc. NUTS software.</span> | **** <span style="text-decoration:line-through;">Acorn NMR Inc. NUTS software.</span> | ||
**** <span style="text-decoration:line-through;">ACD/Labs NMR Processor software.</span> | **** <span style="text-decoration:line-through;">ACD/Labs NMR Processor software.</span> | ||
<br/> | <br/> | ||
| − | + | ==== NMR Database ==== | |
* [http://nmrshiftdb.nmr.uni-koeln.de/nmrshiftdb/media-type/html/user/anon/page/default.psml/js_pane/P-Home nmrshiftdb2] | * [http://nmrshiftdb.nmr.uni-koeln.de/nmrshiftdb/media-type/html/user/anon/page/default.psml/js_pane/P-Home nmrshiftdb2] | ||
"nmrshiftdb2 is a NMR database (web database) for organic structures and their nuclear magnetic resonance (nmr) spectra. It allows for spectrum prediction (13C, 1H and other nuclei) as well as for searching spectra, structures and other properties. Last not least, it features peer-reviewed submission of datasets by its users. The nmrshiftdb2 software is open source, the data is published under an open content license. Please consult the [http://nmrshiftdb.nmr.uni-koeln.de/portal/js_pane/P-Help documentation] for more detailed information. nmrshiftdb2 is the continuation of the NMRShiftDB project with additional data and bugfixes and changes in the software." | "nmrshiftdb2 is a NMR database (web database) for organic structures and their nuclear magnetic resonance (nmr) spectra. It allows for spectrum prediction (13C, 1H and other nuclei) as well as for searching spectra, structures and other properties. Last not least, it features peer-reviewed submission of datasets by its users. The nmrshiftdb2 software is open source, the data is published under an open content license. Please consult the [http://nmrshiftdb.nmr.uni-koeln.de/portal/js_pane/P-Help documentation] for more detailed information. nmrshiftdb2 is the continuation of the NMRShiftDB project with additional data and bugfixes and changes in the software." | ||
<br/> | <br/> | ||
| − | ====== '''General | + | <br/> |
| − | + | ==== Support ==== | |
| − | + | {| class="wikitable" | |
| − | + | |+ '''Agilent General Customer Support''' | |
| − | + | ! Contact !! Telephone Number | |
| + | |- | ||
| + | | align="Left" | Customer Service | ||
| + | | align="Right" | 1-800-227-9770 option 3 then option 7 | ||
| + | |- | ||
| + | |} | ||
| + | <br/> | ||
| + | NMR Lab Room (Lab I 2033) Telephone #: 360-867-'''7783''' | ||
<br/> | <br/> | ||
<br/> | <br/> | ||
Latest revision as of 10:01, 8 August 2022
Nuclear Magnetic Resonance Spectroscopy Wikipedia entry
Manuals
Information Table
Contents
Notes
- WARNING: STRONG MAGNETIC FIELD!
- Read all warnings posted near instrument.
- The NMR has a hardware console. The PC connects to the NMR console via ethernet cable.
- The PC is configured with a dedicated private [172.16.0.0/24] network on eth1/eno1.
- eth2/eno2 is on TESC LAN w/ static IP 10.15.10.6
- Student access to the PC:
- UN: student
- PW: student1
- Network Information
- PC is not joined to the domain;
- There's a shortcut on the desktop [called NMR-Data] to \\Orca\research\NMR-Data [this is a 'static' connection using the scuser domain account]
- The reference hardware/software serial #: S010780
- The software (OpenVnmrJ) will create raw free induction decay (FID) files
- These files can be directed to the network share by browsing to \Home\student\desktop\NMR-Data
- VnmrJ Issues/Bugs:
- If the software is closed by clicking on the window x icon to close the application, VnmrJ will leave behind a lock file within the users profile.
- The issue/Bug will be experienced if the user tries to open the application again, and tries to start a new test, VnmrJ will display an error.
- Assuming that the user is "Student", the lock file will be found in this directory: \Home\Student\VNMRsys
- the lock file will have a .primary file extension as well as having "lock" in the file name;
- for example: rm_lock_4.primary
- in the example, the 4 will represent the "4" or "4th" test.
- Printer Configuration
- printer setup within VNMRJ administration, requires that the printer be configured with emulation, specifically Laser Jet 600R has been found to be a good configuration that will utilize the entire 8 1/2 x 11 page for plotter.
General instrument information
- The helium needs to be recharged every 4 month [MAX believed to be 6 months]
- The liquid nitrogen needs to be recharged every 1 week [Max is believed to be 2 weeks]
- Consequence of failure to recharge aformentioned gases is "Magnetic Quench"!
- It's estimated that it would/will cost $15K to fix should quench occur.
NMR Spectroscopy Software
NMR Database
"nmrshiftdb2 is a NMR database (web database) for organic structures and their nuclear magnetic resonance (nmr) spectra. It allows for spectrum prediction (13C, 1H and other nuclei) as well as for searching spectra, structures and other properties. Last not least, it features peer-reviewed submission of datasets by its users. The nmrshiftdb2 software is open source, the data is published under an open content license. Please consult the documentation for more detailed information. nmrshiftdb2 is the continuation of the NMRShiftDB project with additional data and bugfixes and changes in the software."
Support
| Contact | Telephone Number |
|---|---|
| Customer Service | 1-800-227-9770 option 3 then option 7 |
NMR Lab Room (Lab I 2033) Telephone #: 360-867-7783
