NMR

From Help Wiki
Revision as of 12:33, 30 November 2012 by Geeraerd (Talk | contribs) (Created page with '<!-- NMR Instrument Page --> NMR <br/> <br/> [http://en.wikipedia.org/wiki/NMR Nuclear Magnetic Resonance Spectroscopy Wikipedia entry] <b…')

(diff) ← Older revision | Latest revision (diff) | Newer revision → (diff)

NMR

Nuclear Magnetic Resonance Spectroscopy Wikipedia entry

Manual

Information Schema


Notes
  • WARNING: STRONG MAGNETIC FIELD!
    • Read all warnings posted near instrument.
  • The NMR has a hardware console. The PC connects to the NMR console via ethernet cable.
    • The PC is configured with a dedicated private [10.10.] network.on eth1.
    • eth0 is on TESC LAN w/ static IP 10.14.3.200
  • Student access to the PC:
    • UN: student
    • PW: c13nmr
  • Network Information
    • PC is not joined to the domain;
    • If accessing resources on TESC LAN network, and credentials are required, when prompted for "domain name" use AC_COMPUTING [this is the legacy Windows NETBIOS name]
    • There's a shorcut on the desktop [called NMR-Data-to-Orca] to \\Orca\research\NMR-Data [this is a 'static' connection using the acuser domain account]
  • The reference hardware/software serial #: S010780
  • The software (VnmrJ 2.2D) license codes
    • G5023AA
    • G5027AA
  • The software (VnmrJ) will create raw free induction decay [(FID)] files
    • These files can be directed to the network share by browsing to \Home\student\desktop\NMR-Data-to-Orca
      • These raw FID files can be read by Acorn NMR Inc. NUTS software.
      • These raw FID files can be read by ACD NMR Processor software.
        • The CAL has this software installed.
    • Help files/Manuals are located on the desktop
      • /home/student/desktop/VnmrJ_Manual/
  • VnmrJ Issues/Bugs:
    • If the software is closed by clicking on the window x icon to close the application, VnmrJ will leave behind a lock file within the users profile.
    • The issue/Bug will be experienced if the user tries to open the application again, and tries to start a new test, VnmrJ will display an error.
      • Assuming that the user is "Student", the lock file will be found in this directory: \Home\Student\VNMRsys
      • the lock file will have a .primary file extension as well as having "lock" in the file name;
        • for example: rm_lock_4.primary
        • in the example, the 4 will represent the "4" or "4th" test.
  • General instrument information
    • The helium needs to be recharged every 4 month [MAX believed to be 6 months]
    • The liquid nitrogen needs to be recharged every 1 week [Max is believed to be 2 weeks]
    • Consequence of failure to recharge aformentioned gases is ["Magnetic Quench"!]
      • It's estimated that it would/will cost $15K to fix should quench occur.




back to Main page